Extraction Of Brazilin From Sappan Wood as a Natural Reagent for Borax Detection by Digital Imaging Analysis
Abstract
The use of brazilien for borax detection is because the chemical properties of this compound are greatly influenced by pH which results in a change in the color of the brazilien. This compound gives an orange color at a pH range of 6-7 and yellow at an acidic pH, while at a pH range of 7-10 it gives a red color and at a pH >10 it gives a purplish red color. This research uses Brazilian extract from sappan wood for borax detection. By utilizing this compound extract, the use of chemical reagents for the detection of borax in food samples can be minimized. Apart from that, it can increase the added value of these crop commodities and can take advantage of the abundant natural resources in Indonesia. This research aims to develop a method that is accurate, simple and cheap and does not use special instruments to diagnose borax based on digital imaging, which includes extraction of brazilien from sappan wood using a maceration method using 96% ethanol solvent and water with a UV-Vis spectrophotometer, ratio optimization brazilin extract with boric acid, optimization of measurement time. The results of the research show that the solvent that provides optimum absorbance for brazilin extraction is water or distilled water, with a ratio of brazilin extract and boric acid of 1:1 and the measurement time is 5 minutes.
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References
Ataide, V. N., Mendes, L. F., Gama, L. I., de Araujo, W. R., & Paixão, T. R. (2020). Electrochemical paper-based analytical devices: ten years of development. Analytical Methods, 12(8), 1030-1054.
Noviana, E., Ozer, T., Carrell, C. S., Link, J. S., McMahon, C., Jang, I., & Henry, C. S. (2021). Microfluidic paper-based analytical devices: from design to applications. Chemical reviews, 121(19), 11835-11885.
Noviana, E., Carrão, D. B., Pratiwi, R., & Henry, C. S. (2020). Emerging applications of paper-based analytical devices for drug analysis: A review. Analytica chimica acta, 1116, 70-90.
Marquez, S., & Morales-Narváez, E. (2019). Nanoplasmonics in paper-based analytical devices. Frontiers in Bioengineering and Biotechnology, 7, 69.
Wang, C. M., Chen, C. Y., & Liao, W. S. (2021). Enclosed paper-based analytical devices: Concept, variety, and outlook. Analytica Chimica Acta, 1144, 158-174.
Kresnadipayana, D., D.Lestari. (2017). Determination Of Borax Level On Dates (Phoenix Dactylifera) With Uv-Vis Spectrophotometric Method. Jurnal Wiyata, Vol. 4 No. 1, 23-30.
Nisa, K. A. (2020). Monitoring Kemunduran Mutu Semangka Potong Menggunakan Kemasan Pintar Berindikator Ekstrak Kayu Secang (Caesalpinia Sappan l.) (Doctoral dissertation, Politeknik Negeri Jember).
Ozer, T., McMahon, C., & Henry, C. S. (2020). Advances in paper-based analytical devices. Annual Review of Analytical Chemistry, 13(1), 85-109.
Putri, Umasari Sihmentari., Ana Hidayati Mukharomah., Ayu Rahmawati., Sulistyaningtyas. (2018). Pengaruh Konsentrasi Pelarut Etanol terhadap Absorbansi Brazilin pada Simplisia Kayu Sappan (Caesalpinia sappan L.). rosiding Seminar Nasional Mahasiswa Unimus Vol. 1
Rahayuningsih, Edia., Wiratni Budhijanto., Hana Fitria Prasasti, and Meyta Tias Wahyuningrum. (2018). Chemical Modifications for Intensity Variation and Spectrum Extension of Brazilein Extract from Sappanwood (Caesalpinia sappan L.). MATEC Web of Conferences 156, 01020. doi.org/10.1051/matecconf/201815601020
Rosyida, N, L Dinira and E R N Wulandari. (2020). The possibility of smartphone camera to determine iron(III) in solution, IOP Conf. Series: Materials Science and Engineering 801 (2020) 012133. doi:10.1088/1757-899X/801/1/012133
Siriangkhawut, W., Khanhuathon, Y., Chantiratikul, P., Ponhong, K., Grudpan, K. (2016). A Green Sequential Injection Spectrophotometric Approach Using Natural Reagent Extracts from Heartwood of Ceasalpinia sappan Linn. for Determination of Aluminium. Anal Sci. 32(3), 329-36. doi: 10.2116/analsci.32.329. PMID: 26960614.
Ulma, Zeni., Edia Rahayuningsih., Tutik Dwi Wahyuningsih. (2017). Methylation of Brazilein on Sappan (Caesalpinia sappan Linn) Wood Extract for Maintain Color Stability to the Changes of pH, IOP Conf. Series: Materials Science and Engineering 299 (2017) 012075, doi:10.1088/1757-899X/299/1/012075
Wahyuni., Reny Sri. (2020). Uji Kualitas Ekstrak Kulit Sappan (Caesalpinia Sappan L.) Sebagai Kandidat Borax Rapid Test Kit. Diploma III Analisis Kimia. Fakultas Matematika Dan Ilmu Pengetahuan Alam, Universitas Islam Indonesia
Robbani, S., Elya, B., & Iswandana, R. (2022). Alpha-glucosidase and DPP-IV inhibitory activities of ethanol extract from caesalpinia sappan, andrographis paniculata, and syzygium cumini. Pharmacognosy Journal, 14(3).
Failisnur, F., Sofyan, S., & Silfia, S. (2019). Ekstraksi kayu secang (Caesalpinia sappan Linn) dan aplikasinya pada pewarnaan kain katun dan sutera. Indonesian Journal of Industrial Research, 9(1), 33-40.
Sari, N., Rachma & Santi (2017). Potensi Zat Warna dari Ekstrak Etanol Kayu Sappang Sebagai KalorimetriAnion. Al-Kimia, 5 (2), 136-144
Misbah, S. R., Darmayani, S., & Nasir, N. (2018). Analisis kandungan boraks pada bakso yang dijual di anduonohu kota kendari sulawesi tenggara. Jurnal Kesehatan Manarang, 3(2), 81-85
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